THERMAL BEHAVIOUR OF LAYERED ORGANIC-INORGANIC NANOCOMPOSITE: BETA-NAPHTOXYACETIC ACID INTERCALATED INTO ZINC-ALUMINIUM LAYERED DOUBLE HYDROXIDE

Authors

  • Zaemah Jubri Department of Science & Mathematics, College of Engineering, Universiti Tenaga Nasional, 43009 Kajang, Selangor, Malaysia Author
  • Nor Zalina Anua Mohd Yusoff Department of Science & Mathematics, College of Engineering, Universiti Tenaga Nasional, 43009 Kajang, Selangor, Malaysia Author
  • Siti Halimah Sarijo Faculty of Applied Science, Universiti Teknologi Mara, 40450 Shah Alam, Selangor, Malaysia Author
  • Elya Sufliza Marsom Department of Science and Mathematics, Universiti Tun Hussein Onn Malaysia, 86400 Parit Raja, Batu Pahat, Johor, Malaysia Author

Keywords:

Zn-Al-BNOA, nanocomposite, microstructure

Abstract

An organic-inorganic nanohybrid material of zinc-aluminium-layered double hydroxide containing beta-naphtoxyacetic acid (BNOA) as the interlamella anion was synthesized using co-prepitation method. BNOA ion was successfully intercalated into Zn-Al layered double hydroxide by expanding the interlayer spacing from 8.93 Å to 19.46 Å based on the PXRD diffractogram of the nanocomposite. Thermal composition (calcination) of the nanocomposite (Zn-Al-BNOA) was studied by heating the samples at 100 – 800 °C under atmospheric condition. The layered structure of the nanocomposite collapsed when the sample was heated at 350 °C and the formation of ZnO phase was observed at 400 °C and higher. Further characterization for the FTIR and organic-inorganic composition and SEM, were also carried out.

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Published

23-05-2026

How to Cite

Zaemah Jubri, Nor Zalina Anua Mohd Yusoff, Siti Halimah Sarijo, & Elya Sufliza Marsom. (2026). THERMAL BEHAVIOUR OF LAYERED ORGANIC-INORGANIC NANOCOMPOSITE: BETA-NAPHTOXYACETIC ACID INTERCALATED INTO ZINC-ALUMINIUM LAYERED DOUBLE HYDROXIDE. Solid State Science and Technology, 19(1), 107-113. https://journal.massmalaysia.org/ojs/index.php/ssst/article/view/1